Enhanced flavour extraction in continuous liquid-liquid extractors.

نویسندگان

  • Peter Apps
  • Margaux Lim Ah Tock
چکیده

Continuous liquid-liquid extraction is a versatile, reliable and robust sample preparation technique, but there is a tendency for the solvent to make channels through the sample, causing uneven and incomplete extraction. A simple, cheap magnetic stirrer that prevents channelling improves extraction efficiency by between 2.8 and 17.6 times.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Studies of Drop Behavior and Prediction of Sauter Mean Drop Diameter in Various Rotary Agitated Extraction Columns

Knowledge of droplet behavior is one of the most important criteria for determination of mass transfer kinetics for choosing the type of liquid-liquid extraction columns. Mean drop size data of dispersed phase droplets in continuous phase have been obtained for Various Rotary Agitated Liquid-Liquid Extraction Columns . The effects of operational variables such as mass transfer directions with a...

متن کامل

Investigation of Mass Transfer Coefficient under Jetting Conditions in a Liquid-Liquid Extraction System

In this research mass transfer coefficient under jetting regime in different directions (from dispersed to continuous and continuous to dispersed phase) has been studied using an experimental setup. n-Butanol-succinic acid-water with low interfacial tension has been selected as experimental chemical system. The effects of various parameters such as jet velocity, nozzle diameter and the heig...

متن کامل

Ionic Liquid Based Dispersive Liquid Liquid Microextraction and Enhanced Determination of the Palladium in Water, Soil and Vegetable Samples by FAAS

In this study, we combined Ionic Liquid-based Dispersive Liquid Liquid Micro Extraction (IL-DLLME) with FAAS for determining the palladium in different real samples at the trace level. 1-hexyl-3-methylimidazolium hexafluorophosphate [Hmim][PF6] ionic liquid and 1-(2-pyridylazo) 2-naphthol (PAN), were chosen as the extraction solvent and the chelating agent, respectively. The hydr...

متن کامل

Stagewise Modeling of Liquid-Liquid Extraction Column (RDC)

Stagewise forward mixing model considering coalescence and redispersion of drops was used to predict the performance of Rotating Disc Liquid-Liquid Extraction Contactors. Experimental data previously obtained in two RDC columns of 7.62cm diameter, 73.6cm height and 21.9cm diameter, 150cm height were used to evaluate the model predictions. Drop-side mass transfer coefficients were predicted appl...

متن کامل

Optimization of batch to continuous transposition: solid-liquid extraction from plant in an industrial contactor

Solid-liquid extraction is carried out from vegetable substrates in industrial continuous counter-current extractor. A batch study was conducted to obtain the extraction kinetic and the bulk phase saturation. An extraction model is proposed and compared with experimental data. This model is based on the general diffusion model including a shape factor of solid particle. A methodology for the ba...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Journal of chromatography. A

دوره 1083 1-2  شماره 

صفحات  -

تاریخ انتشار 2005